HRID1020736
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of 4-[2-(3-Chloro-benzylamino)-quinoxalin-6-yl]-pyrazole-1-carboxylic acid tert-butyl ester (0.35 g, 0.80 mmol) in DCM (4 mL), was added HCl in dioxane (0.4 mL) at room temperature. After completion of the reaction, the reaction mixture was concentrated and washed with DCM (4 mL) to obtain the title compound (0.06 g, 22%).
WORKUP
后处理
- customAfter completion of the reaction
- concentrationthe reaction mixture was concentrated
- washwashed with DCM (4 mL)