HRID1024453

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID73768

1-Isocyanato-4-(trifluoromethyl)benzene

C8H4F3NO

结构：COC(=O)C(NC(=O)c1nc(-c2ccc([N+](=O)[O-])cc2)cs1)C(C)C

HCID67150325

未命名化合物

PRODUCTS

生成物

结构：COC(=O)C(NC(=O)c1nc(-c2ccc(NC(=O)Nc3ccc(C(F)(F)F)cc3)cc2)cs1)C(C)C

HCID52935054

未命名化合物

收率 79%

PROCEDURE

实验过程

The title compound was synthesized analogous to Example 23, using 1-isocyanato-4-(trifluoromethyl)benzene and intermediate 3. Yield: 79%; 1H NMR (DMSO-d6, 300 MHz): δ 9.14 (s, 1H), 8.99 (s, 1H), 8.80 (d, 1H), 8.32 (s, 1H), 8.06 (d, 2H), 7.66 (bs, 4H), 7.61 (d, 2H), 4.37 (s, 1H), 3.70 (s, 3H), 2.32 (m, 1H), 0.97 (s, 6H).