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HRID1025293

反应详情

EQUATION

反应方程式

HRID 1025293 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC[C@H](NC(=O)OC(C)(C)C)[C@H](O)C(=O)NC1CC1
HCID86762402

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@H](N)[C@H](O)C(=O)NC1CC1.Cl.Cl
HCID86762404

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

Under an atmosphere of argon, tert-butyl (2S,3S)-1-(cyclopropylamino)-2-hydroxy-1-oxopentan-3-ylcarbamate (540 mg, 1.98 mmol) and HCl 4N in dioxane (10.4 ml) were combined to give a light brown solution. The reaction was stirred for 4 h at RT. The solvent was evaporated. The residual solvent was removed under vacuum. The title compound was obtained as a brown solid (480 mg, quant., MS (m/e)=173.2 [M+H+].

WORKUP

后处理

  1. customto give a light brown solution
  2. customThe solvent was evaporated
  3. customThe residual solvent was removed under vacuum