HRID1026671

反应详情

EQUATION

反应方程式

HRID 1026671 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound was prepared by reacting (S)—N-{3-[4-(4-oxopiperidin-1-yl)-3-fluorophenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide (12.0 mmol) and potassium cyanide (18.0 mmol) in dimethylformamide (25 ml) at a temperature 25° C. for four hours and by purifying the compound by silica gel column chromatography in 42% yield.

WORKUP

后处理

  1. customat a temperature 25° C.
  2. customfor four hours
  3. customby purifying the compound by silica gel column chromatography in 42% yield