Oleylamine → HCID 178442897, compound

HRID 1029341Notes

Reaction equation

HRID 1029341 reaction equation
[SH:1][C:2]1[S:3][C:4]([S:7][CH:8]2[CH2:13][C:12](=[O:14])O[C:9]2=[O:10])=[N:5][N:6]=1.[CH2:15]([NH2:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32]>C1(C)C(C)=CC=CC=1>[CH2:15]([N:33]1[C:12](=[O:14])[CH2:13][CH:8]([S:7][C:4]2[S:3][C:2]([SH:1])=[N:6][N:5]=2)[C:9]1=[O:10])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32]

Participants

4

Reactant 2

HCID 5356789OleylamineHCID 178516660HCID 178516660, compound

Product 1

HCID 178442897HCID 178442897, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

A mixture of 2-(2-mercapto-1,3,4-thiadiazol-5-ylthio)-succinic anhydride and oleylamine (1:1 molar ratio) in xylene was refluxed for three hours. After removing the solvent under reduced pressure, the reaction product was a light brown, viscous oil. Both its IR spectrum and elemental analysis appeared to be consistent with the proposed structure. A sample of N-(2-ethylhexyl)-2-(2-mercapto-1,3,4-thiadiazol-5-ylthio)-succinimide was similarly prepared.

Workup

  1. temperaturewas refluxed for three hours
  2. customAfter removing the solvent under reduced pressure
  3. customA sample of N-(2-ethylhexyl)-2-(2-mercapto-1,3,4-thiadiazol-5-ylthio)-succinimide was similarly prepared

Sources & evidence

ORD record
ord-517d59bfddde493b9a12a50da3cac887
Source dataset
uspto-grants-1992_04
Patent number
US05102568

Reaction notes

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