反应详情

A mixture of 2-(2-mercapto-1,3,4-thiadiazol-5-ylthio)-succinic anhydride and oleylamine (1:1 molar ratio) in xylene was refluxed for three hours. After removing the solvent under reduced pressure, the reaction product was a light brown, viscous oil. Both its IR spectrum and elemental analysis appeared to be consistent with the proposed structure. A sample of N-(2-ethylhexyl)-2-(2-mercapto-1,3,4-thiadiazol-5-ylthio)-succinimide was similarly prepared.

1. temperaturewas refluxed for three hours
2. customAfter removing the solvent under reduced pressure
3. customA sample of N-(2-ethylhexyl)-2-(2-mercapto-1,3,4-thiadiazol-5-ylthio)-succinimide was similarly prepared