HRID1030419

反应详情

EQUATION

反应方程式

HRID 1030419 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Following the same procedure as described in Preparation 18, 2 g of 6-acetoxy-2-(4-aminophenoxymethyl)-2,5,7,8-tetramethylchroman (prepared as described in Preparation 50), 25 ml of acetone, 3 ml of 35% w/v aqueous hydrochloric acid, 0.7 g of sodium nitrite, 1 ml of water, 8 g of ethyl methacrylate and 0.2 g of cuprous oxide were reacted, to give the title compound.

WORKUP

后处理

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