Thioglycolic Acid → HCID 14999087, compound

HRID 1030552Notes

Reaction equation

HRID 1030552 reaction equation
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1.[CH3:9][NH2:10].[C:11]([OH:15])(=O)[CH2:12][SH:13]>>[CH3:9][N:10]1[C:11](=[O:15])[CH2:12][S:13][CH:1]1[C:2]1[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 1133Thioglycolic AcidHCID 6329MethylamineHCID 103713-Pyridinecarboxaldehyde

Product 1

HCID 14999087HCID 14999087, compound

Procedure

According to the procedure of Example 3, the title compound was prepared by using nicotinaldehyde, a 40% aqueous methylamine solution, and thioglycolic acid as charge stock. m.p. 96.5°-97.5° C. IR (nujol) [cm-1 ]; 1670, 1583, 1236, 1109, 1005, 717.

Sources & evidence

ORD record
ord-b91f98d7d53f496b9c070bea6ca91598
Source dataset
uspto-grants-1992_04
Patent number
US05106860

Reaction notes

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