Hydrochloric Acid → HCID 131717326, compound

HRID 1031216Notes

Reaction equation

HRID 1031216 reaction equation
[ClH:1].Cl.Cl.Cl.[CH2:5]([NH:7][CH2:8][CH2:9][CH2:10][NH:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][NH:20][CH2:21][CH2:22][CH2:23][NH:24][CH2:25][CH3:26])[CH3:6].Cl.C([OH:30])C>C(OCC)C>[OH2:30].[ClH:1].[ClH:1].[ClH:1].[ClH:1].[CH2:25]([NH:24][CH2:23][CH2:22][CH2:21][NH:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][NH:11][CH2:10][CH2:9][CH2:8][NH:7][CH2:5][CH3:6])[CH3:26].[CH2:25]([NH:24][CH2:23][CH2:22][CH2:21][NH:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][NH:11][CH2:10][CH2:9][CH2:8][NH:7][CH2:5][CH3:6])[CH3:26].[ClH:1].[ClH:1].[ClH:1].[ClH:1]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 14585895HCID 14585895, compound

Product 1

HCID 131717326HCID 131717326, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Dissolve 3.3 g (0.0046 mol) of the product of Step A in 7 ml ethanol and treat with 70 ml of 2 N HCl in diethyl ether stirring overnight. Filter the mixture and dry the residue at 70° C. at reduced pressure to yield 1.95 g of the title 46.09, H-10.10, N-11.95, Cl-30.24; Found C-46.23, H-9.94, N-12.11, Cl-29.99.

Workup

  1. filtrationFilter the mixture
  2. customdry the residue at 70° C. at reduced pressure
  3. customto yield 1.95 g of the title 46.09, H-10.10

Sources & evidence

ORD record
ord-ba82332288cb45b9b60f6288e13a5e54
Source dataset
uspto-grants-1992_04
Patent number
US05109024

Reaction notes

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