Hydrochloric Acid → HCID 14585894, compound

HRID 1031217Notes

Reaction equation

HRID 1031217 reaction equation
[CH2:1]([N:3](C(OC(C)(C)C)=O)[CH2:4][CH2:5][CH2:6][N:7](C(OC(C)(C)C)=O)[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][N:16](C(OC(C)(C)C)=O)[CH2:17][CH2:18][CH2:19][NH:20]C(OC(C)(C)C)=O)[CH3:2].[ClH:49]>C(O)C.C(OCC)C>[ClH:49].[ClH:49].[ClH:49].[ClH:49].[NH2:20][CH2:19][CH2:18][CH2:17][NH:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][NH:7][CH2:6][CH2:5][CH2:4][NH:3][CH2:1][CH3:2]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 14585892HCID 14585892, compound

Product 1

HCID 14585894HCID 14585894, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 3283Diethyl EtherSolvent

Procedure

Dissolve 2.5 g (0.0036 mol) of the product of Step A in 5 ml of ethanol and treat with 60 ml of 2 N HCl in diethyl ether stirring overnight. Filter the mixture and dry the residue to yield 1.35 g of the title compound, mp >300° C. Elemental analysis: Calculated, C-43.54, H-9.82, N-12.69, Cl-32.13; Found, C-43.43, H-9.60, 9.55; N-12.60, 12.62; Cl-32.30.

Workup

  1. filtrationFilter the mixture
  2. customdry the residue

Sources & evidence

ORD record
ord-1f309a75ac6f4929b00c243577966da2
Source dataset
uspto-grants-1992_04
Patent number
US05109024

Reaction notes

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