Aniline → 4-Nitro-N-phenylbenzenesulfonamide

HRID 1031292Notes

Reaction equation

HRID 1031292 reaction equation
Nc1ccccc1.O=[N+]([O-])c1ccc(S(=O)(=O)Cl)cc1>CC(C)=O.O.O=C([O-])O.OCCOCCOCCOCCOCCO.[Na+]>O=[N+]([O-])c1ccc(S(=O)(=O)Nc2ccccc2)cc1

Participants

7

Reactant 2

HCID 6115AnilineHCID 74044-Nitrobenzenesulfonyl chloride

Product 1

HCID 3137214-Nitro-N-phenylbenzenesulfonamideYield 98%

Reagents, catalysts & solvents 4

HCID 516892Sodium BicarbonateReagentHCID 180AcetoneSolventHCID 962WaterSolventHCID 62551Pentaethylene glycolSolvent

Conditions

Temperature
25 °C

Workup

  1. additionNo procedure recorded
  2. extractionKeep organic
  3. washNo procedure recorded
  4. washNo procedure recorded
  5. dry with materialNo procedure recorded
  6. concentrationNo procedure recorded

Sources & evidence

ORD record
ord-2d9744b45378425790df1ae6c2ee2c57
Source dataset
39 compound library from "Building a Sulfonamide Library by Eco-Friendly Flow Synthesis"
Original link
View source

Reaction notes

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