HRID1032018

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C(O)Cc1c(F)cc2c(=O)c(C(=O)O)cn(C3CC3)c2c1F

HCID14422913

未命名化合物

PRODUCTS

生成物

结构：Cc1c(F)cc2c(=O)c(C(=O)O)cn(C3CC3)c2c1F

HCID13657423

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID7583

Diphenyl oxide

C12H10O

PROCEDURE

实验过程

0.5 g of the compound from Example 11 is heated to 240° C. for one hour in 5 ml of diphenyl ether. The residue remaining after distilling off the solvent consists of 0.3 g of crude product of melting point 208°-10° C. Recrystallization from ethanol gives a melting point of 226°-28°.

WORKUP

后处理

distillationafter distilling off the solvent
customRecrystallization from ethanol
customgives a melting point of 226°-28°