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HRID1038078

反应详情

EQUATION

反应方程式

HRID 1038078 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COC(=O)C1(C(C)OC(C)=O)CCN(Cc2ccccc2)C1
HCID57685792

Methyl 3-[1-(acetyloxy)ethyl]-1-(phenylmethyl)-3-pyrrolidinecarboxylate

C17H23NO4

PRODUCTS

生成物

1
结构：COC(=O)C1(C(C)O)CCN(Cc2ccccc2)C1
HCID57686370

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

2M HCl (25 ml) was added to a solution of 3-(1-Acetoxy-ethyl)-1-benzyl-pyrrolidine-3-carboxylic acid methyl ester (2N) (5 g, 16.39 mmol) in MeOH (50 ml) at room temperature, then refluxed for 2 hours. The solvent was evaporated yielding the product (4.39, 100%) ESMS (MH, 264).

WORKUP

后处理

  1. temperaturerefluxed for 2 hours
  2. customThe solvent was evaporated
  3. customyielding the product (4.39, 100%) ESMS (MH, 264)