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HRID10426

反应详情

EQUATION

反应方程式

HRID 10426 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CSc1ccccc1
HCID7520

Benzene, (methylthio)-

C7H8S

结构：CC(C)(C)OC(=O)N[C@@H]1C[C@@H]2CC[C@@H](C#N)N2C1=O
HCID91321587

未命名化合物

PRODUCTS

生成物

1
结构：N#C[C@@H]1CC[C@H]2C[C@@H](N)C(=O)N21.O=C(O)C(F)(F)F
HCID11357934

未命名化合物

PROCEDURE

实验过程

80 mg of tert-butyl ((2R,5S,7aS)-5-cyano-3-oxohexahydropyrrolizin-2-yl)carbamate were C reacted with 10% thioanisole in 1 ml of trifluoroacetic acid for 30 min. The solvents were then removed in vacuo, and the residue was stirred with diusopropyl ether.

WORKUP

后处理

  1. customThe solvents were then removed in vacuo