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HRID1044089

反应详情

EQUATION

反应方程式

HRID 1044089 的结构方程式

REACTANTS

反应物

3
结构：CI
HCID6328

Methyl iodide

CH3I

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：CC1(C)CN(C2CCCC2)c2nc(Cl)ncc2NC1=O
HCID58154012

未命名化合物

PRODUCTS

生成物

1
结构：CN1C(=O)C(C)(C)CN(C2CCCC2)c2nc(Cl)ncc21
HCID59295116

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Reaction of 2-chloro-9-cyclopentyl-7,7-dimethyl-5,7,8,9-tetrahydro-pyrimido[4,5-b][1,4]diazepin-6-one with MeI and NaH in DMF gave 2-chloro-9-cyclopentyl-5,7,7-trimethyl-8,9-dihydro-5H-pyrimido[4,5-b][1,4]diazepin-6(7H)-one