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HRID1044340

反应详情

EQUATION

反应方程式

HRID 1044340 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)N1CCCC2(CCN([C@H]3CC[C@@H](O)CC3)C2=O)C1
HCID178451763

未命名化合物

PRODUCTS

生成物

1
结构：Cl.O=C1N([C@H]2CC[C@@H](O)CC2)CCC12CCCNC2
HCID178479651

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Hydrogen chloride (2.0 mL, 4.0 M in 1,4-dioxane) was added to a solution of tert-butyl 2-(cis-4-hydroxycyclohexyl)-1-oxo-2,7-diazaspiro[4.5]decane-7-carboxylate (0.10 g) in ethyl acetate (0.5 mL) at room temperature and the mixture was stirred for 1 h. The solvent was then removed under vacuum to give the product. LC-MS: 253.2 (M+H)+.

WORKUP

后处理

  1. customThe solvent was then removed under vacuum
  2. customto give the product