HRID1046041

反应详情

EQUATION

反应方程式

HRID 1046041 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To 1000 ml of ethanol was added 120 g of Lamivudine oxalate (prepared by the method of the present invention). 60 ml of triethylamine was added thereto at the temperature of 40˜45° C. for 0.5 hour, and stirred at the same temperature for 4 hours. The mixture was centrifuged at room temperature and dried under vacuum at the temperature of 40˜45° C. to obtain Lamivudine crystal.

WORKUP

后处理

  1. customprepared by the method of the present invention)
  2. customwas centrifuged at room temperature
  3. customdried under vacuum at the temperature of 40˜45° C.