HRID1046041
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To 1000 ml of ethanol was added 120 g of Lamivudine oxalate (prepared by the method of the present invention). 60 ml of triethylamine was added thereto at the temperature of 40˜45° C. for 0.5 hour, and stirred at the same temperature for 4 hours. The mixture was centrifuged at room temperature and dried under vacuum at the temperature of 40˜45° C. to obtain Lamivudine crystal.
WORKUP
后处理
- customprepared by the method of the present invention)
- customwas centrifuged at room temperature
- customdried under vacuum at the temperature of 40˜45° C.