Ethanol → HCID 68479385、化合物
反応式
C[O:2][C:3]([C:5]1[CH:13]=[C:12]2[C:8]([C:9]([CH2:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)([CH3:15])[C:10](=[O:14])[NH:11]2)=[CH:7][CH:6]=1)=[O:4].[OH-].[Na+].C(O)C.O>O1CCCC1>[CH2:16]([C:9]1([CH3:15])[C:8]2[C:12](=[CH:13][C:5]([C:3]([OH:4])=[O:2])=[CH:6][CH:7]=2)[NH:11][C:10]1=[O:14])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1参加物
6
実験手順
In a manner similar to that of Example 1C, by reacting 3-Benzyl-3-methyl-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester (1.06 mmol) obtained in Example 19(B), sodium hydroxide (260 mg, 6.5 mmol), ethanol (10 ml) and water (1 ml) in tetrahydrofuran (10 ml), expected derivative was obtained as a white solid.
後処理
- customexpected derivative was obtained as a white solid
出典と根拠
- ORDレコード
- ord-6ff74a2dbc094b2f9f21a68186e786cd
- 出典データセット
- uspto-grants-2016_07
- 特許番号
- US09394267B2
反応ノート
読み込み中…