反应详情

A sample of the compound from step 4 (1.2 g, 6.8 mmol) is hydrogenated (4 atm) in ethanol over 1.2 g of 10% Pd/C for 21.5 hours at room temperature. The mixture is filtered to remove the catalyst, and the solvent is removed to afford the title compound.

1. customfor 21.5 hours
2. customat room temperature
3. filtrationThe mixture is filtered
4. customto remove the catalyst
5. customthe solvent is removed