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HRID1059835

反应详情

EQUATION

反应方程式

HRID 1059835 的结构方程式

REACTANTS

反应物

2
结构：C1CCOC1
HCID8028

Tetrahydrofuran

C4H8O

结构：COc1ccc([N+](=O)[O-])cc1NC(=O)OC(C)(C)C
HCID45790233

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(N)cc1NC(=O)OC(C)(C)C
HCID22344747

tert-Butyl (5-amino-2-methoxyphenyl)carbamate

C12H18N2O3

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of Example 28A in 1:1 THF:methanol (40 mL) was treated with 10% palladium on carbon (800 mg), stirred under hydrogen (1 atm) for one hour, filtered through diatomaceous earth (Celite®), and concentrated to provide the desired product.

WORKUP

后处理

  1. filtrationfiltered through diatomaceous earth (Celite®)
  2. concentrationconcentrated