Gamma-Butyrolactone → HCID 67513941, compound

HRID 1066286Notes

Reaction equation

HRID 1066286 reaction equation
[CH2:1]([NH2:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:20]1(=O)[O:24][CH2:23][CH2:22][CH2:21]1>>[CH2:1]([N:19]1[CH2:20][CH2:21][CH2:22][C:23]1=[O:24])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 7302Gamma-ButyrolactoneHCID 5356789Oleylamine

Product 1

HCID 67513941HCID 67513941, compound

Procedure

Oleylamine (125 g, tech grade, 80% pure, 0.374 mole) was heated with γ-butyrolactone (27 ml, 0.35 mole) at 180° C. under nitrogen for 24 hours. The product was purified via vacuum distillation as a light yellow waxy solid. Mass Spectra: m/e (relative intensity) 335 (M+, 28.40).

Workup

  1. distillationThe product was purified via vacuum distillation as a light yellow waxy solid

Sources & evidence

ORD record
ord-1db405acb1e34980b3a8410ddce50e9e
Source dataset
uspto-grants-2001_06
Patent number
US06242500B1

Reaction notes

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