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HRID1066775

反应详情

EQUATION

反应方程式

HRID 1066775 的结构方程式

REACTANTS

反应物

3
反应SMILES：CN(C)C=O
HCID6228

Dimethylformamide

C3H7NO

反应SMILES：O=C(Cl)C(=O)Cl
HCID65578

Ethanedioyl dichloride

C2Cl2O2

反应SMILES：COc1ccc(C(=O)O)cc1C(F)(F)F
HCID2775295

4-Methoxy-3-(trifluoromethyl)benzoic acid

C9H7F3O3

PRODUCTS

产物

1
反应SMILES：COc1ccc(C(=O)Cl)cc1C(F)(F)F
HCID2775298

4-Methoxy-3-(trifluoromethyl)benzoyl chloride

C9H6ClF3O2

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

The title compound was prepared from 4-methoxy-3-trifluoromethylbenzoic acid with oxalyl chloride and DMF in chloroform at room temperature [D. Levin, Chem. Br., 1977, 20] followed by evaporation in vacuo.

WORKUP

后处理

  1. customfollowed by evaporation in vacuo