HRID1068146

反应详情

EQUATION

反应方程式

HRID 1068146 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound was prepared from 4-benzotriazol-1-yl-piperidine HCl salt and of α-(R)-(3-(R)-formyl-4-(S)-phenylpyrrolidin-1-yl)-cyclohexaneacetic acid, 4-methoxybenzyl ester (prepared above as Aldehyde 5) using procedures analogous to those described in Example 89 Steps C and D except TFA and anisole were used in place of formic acid in Example 89, Step D. ESI-MS 502 (M+1); HPLC A: 2.02 min.

WORKUP

后处理

  1. custom2.02 min.