HRID1069099

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：COC(=O)c1ccc(-c2cccc(NCCN(C[C@H](O[Si](C)(C)C(C)(C)C)c3cccc(Cl)c3)C(=O)OC(C)(C)C)c2)cc1C(=O)OC

HCID69780599

未命名化合物

PRODUCTS

生成物

结构：COC(=O)c1ccc(-c2cccc(NCCNC[C@H](O)c3cccc(Cl)c3)c2)cc1C(=O)OC.Cl.Cl

HCID69780650

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID313

Hydrochloric Acid

ClH

溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

Assay Found: C 55.03; H 5.36; N 5.04%; C26H27Cl1N2O5.0.64H2O requires C 55.04; H 5.38; N 4.94%; from (R)-3′-[[2-[[2-(3-chlorophenyl)-2-[[(tert-butyl)dimethylsilyl]oxy]ethyl][(tert-butoxy)carbonyl]amino]ethyl]amino]-[1,1′-biphenyl]-3,4-dicarboxylic acid dimethyl ester (1.1 g) in 4 N hydrochloric acid in dioxane (10 mL).