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HRID1070770

反应详情

EQUATION

反应方程式

HRID 1070770 的结构方程式

REACTANTS

反应物

2
结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：CC(C)(C)OC(=O)N1CCN(CCN2C(=O)c3ccccc3C2=O)CC1
HCID22397705

tert-Butyl 4-[2-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl]piperazine-1-carboxylate

C19H25N3O4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCN(CCN)CC1
HCID1514400

tert-Butyl 4-(2-aminoethyl)piperazine-1-carboxylate

C11H23N3O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Batch size: 42.2 g (120 mmol) 2-{2-[4-(tert-butoxycarbonyl)-piperazin-1-yl]-ethyl}-isoindolin-1,3-dione and 11.6 ml (240 mmol) hydrazine-hydrate in 450 ml ethanol.