Hydrochloric Acid → HCID 86733473, compound

HRID 1077015Notes

Reaction equation

HRID 1077015 reaction equation
[CH2:1]([O:3][C@H:4]1[CH2:33][C@@:32]2([CH3:34])[C@@H:7]([CH2:8][CH2:9][C@@H:10]3[C@@H:31]2[C:30](=[O:35])[CH2:29][C@@:28]2([CH3:36])[C@H:11]3[CH2:12][CH2:13][C@@H:14]2[C:15](=[O:27])[CH2:16][S:17][C:18](=[O:26])[CH2:19][N:20]2[CH2:25][CH2:24][O:23][CH2:22][CH2:21]2)[CH2:6][C@@H:5]1[OH:37])[CH3:2].[ClH:38]>O>[ClH:38].[CH2:1]([O:3][C@H:4]1[CH2:33][C@@:32]2([CH3:34])[C@@H:7]([CH2:8][CH2:9][C@@H:10]3[C@@H:31]2[C:30](=[O:35])[CH2:29][C@@:28]2([CH3:36])[C@H:11]3[CH2:12][CH2:13][C@@H:14]2[C:15](=[O:27])[CH2:16][S:17][C:18](=[O:26])[CH2:19][N:20]2[CH2:21][CH2:22][O:23][CH2:24][CH2:25]2)[CH2:6][C@@H:5]1[OH:37])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22790342HCID 22790342, compound

Product 1

HCID 86733473HCID 86733473, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

2β-Ethoxy-3α-hydroxy-21-morpholinoacetylthio-5α-pregnane-11,20-dione (134 mg., 0.25 mmole) was dissolved in 0.1 M hydrochloric acid (2.5 ml. 0.25 mmole) and the resulting clear solution was diluted to 13 ml. by the addition of distilled water to give a 1% aqueous solution of the title compound.

Workup

  1. additionthe resulting clear solution was diluted to 13 ml

Sources & evidence

ORD record
ord-e40ef1f70ccc4e8e97fd15d9dfb80f1a
Source dataset
uspto-grants-1976_05
Patent number
US03959260

Reaction notes

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