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HRID1079396

反应详情

EQUATION

反应方程式

HRID 1079396 的结构方程式

REACTANTS

反应物

1
结构：CC(=O)N1CCC(Nc2ccc(N3CCCCC3)cc2)CC1.Cl.Cl
HCID23366978

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Cl.Cl.c1cc(N2CCCCC2)ccc1NC1CCNCC1
HCID23366926

未命名化合物

收率 217.5%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

A solution of 1-acetyl-4-[4-(piperidin-1-yl)phenylamino]piperidine dihydrochloride (0.70 g) in conc. hydrochloric acid (5 ml) was heated with stirring at 100° C. for 15 hours. After the solvent was distilled off, the residue was recrystallized from ethanol to obtain colorless crystals (0.5 g), m.p. 185°-189° C.

WORKUP

后处理

  1. distillationAfter the solvent was distilled off
  2. customthe residue was recrystallized from ethanol