Bromoacetic Acid → HCID 23367206, compound

HRID 1080181Notes

Reaction equation

HRID 1080181 reaction equation
[S:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[Br:6][CH2:7][C:8]([OH:10])=[O:9]>CC(C)=O>[Br-:6].[C:8]([CH2:7][N+:3]1[CH:4]=[CH:5][S:1][CH:2]=1)([OH:10])=[O:9]

Participants

4

Reactant 2

HCID 6227Bromoacetic AcidHCID 9256Thiazole

Product 1

HCID 23367206HCID 23367206, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Thiazole (8.5 g), 2-bromoacetic acid (15.0 g) and acetone (20 ml) were mixed together and left standing at room temperature for 2 days. White crystals deposited were collected by filtration and washed with acetone.

Workup

  1. waitleft
  2. filtrationWhite crystals deposited were collected by filtration
  3. washwashed with acetone

Sources & evidence

ORD record
ord-985f8759db3344389c762bd27e5c394c
Source dataset
uspto-grants-1996_12
Patent number
US05580904

Reaction notes

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