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HRID1084792

反应详情

EQUATION

反应方程式

HRID 1084792 的结构方程式

REACTANTS

反应物

4
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C1CCC(=O)N1Cl
HCID31398

N-Chlorosuccinimide

C4H4ClNO2

结构：ON=Cc1ccc(Cl)cc1
HCID219158

4-Chlorobenzaldehyde oxime

C7H6ClNO

结构：C=CCP(=O)(OCC)OCC
HCID573014

Diethyl allylphosphonate

C7H15O3P

PRODUCTS

生成物

1
结构：CCOP(=O)(CC1CC(c2ccc(Cl)cc2)=NO1)OCC
HCID20062407

未命名化合物

收率 104.5%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Preparation is carried out as in Example 1 from 23.34 g of 4-chlorobenzaldoxime, 22 g of N-chlorosuccinimide, 29.5 g of diethyl allylphosphonate and 22.9 ml of triethylamine in dichloromethane and provides 52 g of oily product.

WORKUP

后处理

  1. customPreparation