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HRID1086180

反应详情

EQUATION

反应方程式

HRID 1086180 的结构方程式

REACTANTS

反应物

3
结构：BrC(c1ccccc1)c1ccccc1
HCID236603

Bromodiphenylmethane

C13H11Br

结构：COc1ccc(COc2cn(O)c(CO)cc2=O)cc1
HCID10707645

未命名化合物

结构：CC(C)(C)[O-].[K+]
HCID23665647

2-Methyl-2-propanol, potassium salt

C4H9KO

PRODUCTS

生成物

1
结构：COc1ccc(COc2cn(OC(c3ccccc3)c3ccccc3)c(CO)cc2=O)cc1
HCID15627767

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

5.54 g of 5-p-methoxybenzyloxy-1-hydroxy-2-hydroxymethyl-4-pyridone is suspended in 40 ml of N,N-dimethylformamide, and then 2.24 g of potassium t-butoxide is added with ice cooling to dissolve. 4.94 g of benzhydryl bromide is added thereto and reacted at room temperature for 2.5 hours.

WORKUP

后处理

  1. dissolutionto dissolve
  2. customreacted at room temperature for 2.5 hours