HRID1087407

反应详情

EQUATION

反应方程式

HRID 1087407 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension containing 22.3 g of 1-bromonaphth-2-ol, 27.75 g of 1-chloro-2,3-epoxypropane and 27.6 g of potassium carbonate in 200 ml of butanone is refluxed overnight. The inorganic salts are filtered off and drained and the filtrate is then evaporated under vacuum. The oil obtained is distilled under 0.01 mm of mercury.

WORKUP

后处理

  1. temperatureis refluxed overnight
  2. filtrationThe inorganic salts are filtered off
  3. customthe filtrate is then evaporated under vacuum
  4. customThe oil obtained
  5. distillationis distilled under 0.01 mm of mercury