Chloroacetone → HCID 15023903, compound

HRID 1090623Notes

Reaction equation

HRID 1090623 reaction equation
[CH3:1][N:2]1[C:10]2[N:9]=[CH:8][N:7]([CH2:11][CH2:12][CH2:13][CH2:14][C:15](=[O:17])[CH3:16])[C:6]=2[C:5](=[O:18])[NH:4][C:3]1=[O:19].Cl[CH2:21][C:22](=[O:24])[CH3:23].C(=O)([O-])[O-].[K+].[K+]>CN(C)C=O>[CH3:1][N:2]1[C:10]2[N:9]=[CH:8][N:7]([CH2:11][CH2:12][CH2:13][CH2:14][C:15](=[O:17])[CH3:16])[C:6]=2[C:5](=[O:18])[N:4]([CH2:21][C:22](=[O:24])[CH3:23])[C:3]1=[O:19]

Participants

5

Reactant 3

HCID 6571ChloroacetoneHCID 11430Potassium CarbonateHCID 19913729HCID 19913729, compound

Product 1

HCID 15023903HCID 15023903, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

This compound was prepared by alkylation of 3-methyl-7-(5-oxohexyl)-xanthine with chloroacetone in dimethylformamide in the presence of potassium carbonate at 100° C. for 1.5 hours.

Sources & evidence

ORD record
ord-887797f0c9a44d7c92208c2aa962dbd5
Source dataset
uspto-grants-1992_01
Patent number
US05082845

Reaction notes

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