反应详情

A mixture of 2-[N-[3-(4-nitrophenoxy)propyl]methylamino methyl]quinoxaline (1.75 g, 4.97 mmol) and PtO2 (0.14 g, 0.62 mmol) in ethanol (170 mL) was charged with 1 atmosphere H2 (g). After 30 minutes, the mixture was filtered through solka floc and concentrated to afford crude product which was purified by HPLC to yield 1.18 g (74%) of a yellow oil.

1. additionwas charged with 1 atmosphere H2 (g)
2. filtrationthe mixture was filtered through solka floc
3. concentrationconcentrated
4. customto afford crude product which
5. customwas purified by HPLC