HRID1091976

反应详情

EQUATION

反应方程式

HRID 1091976 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1 equivalent of pentylmagnesium bromide was reacted with 1 equivalent of the compound obtained in Example 2, in anhydrous THF, under nitrogen, at room temperature. The product thus obtained was worked up and purified on a column of silica. The results of the NMR and mass spectrometry analyses were in accordance with the expected structure.

WORKUP

后处理

  1. customThe product thus obtained
  2. custompurified on a column of silica
  3. customThe results of the NMR and mass spectrometry analyses