Hydrochloric Acid → HCID 18787504, compound

HRID 1107518Notes

Reaction equation

HRID 1107518 reaction equation
[CH2:1]([C:3]1[O:4][C:5]2[C:12]([CH:13]([N:16]([CH2:19][CH3:20])[CH2:17][CH3:18])[CH2:14][OH:15])=[CH:11][CH:10]=[CH:9][C:6]=2[C:7]=1[CH3:8])[CH3:2].[ClH:21]>C(O)(C)C>[ClH:21].[CH2:1]([C:3]1[O:4][C:5]2[C:12]([CH:13]([N:16]([CH2:19][CH3:20])[CH2:17][CH3:18])[CH2:14][OH:15])=[CH:11][CH:10]=[CH:9][C:6]=2[C:7]=1[CH3:8])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 18787505HCID 18787505, compound

Product 1

HCID 18787504HCID 18787504, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

0.79 g (2.86 mmol) of 2-ethyl-3-methyl-7-(1-diethylamino-2-hydroxyethyl)benzofuran and 50 ml of a 0.1N solution of hydrochloric acid in isopropanol are placed in 100 ml round-bottomed flask. The salt is concentrated under vacuum. 0.29 g of 2-ethyl-3-methyl-7-(1-diethylamino-2-hydroxyethyl)benzofuran hydrochloride is obtained in the form of a white wax.

Workup

  1. concentrationThe salt is concentrated under vacuum

Sources & evidence

ORD record
ord-3e3839c7b58c458697085dc729287456
Source dataset
uspto-grants-2000_05
Patent number
US06060508

Reaction notes

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