HRID1108419

反应详情

EQUATION

反应方程式

HRID 1108419 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Under nitrogen atmosphere, a dimethylformamide 100 ml solution of N-bromosuccinimide (22.25 g, 125 mmol) was added dropwise at 0° C. to a dimethylformamide 100 ml solution of 2-tert-butyl-4-methylphenol (20.53 g, 125 mmol) with stirring, the resulting reaction mixture was brought up to room temperature and stirred for 5 hours.

WORKUP

后处理

  1. customthe resulting reaction mixture
  2. customwas brought up to room temperature
  3. stirringstirred for 5 hours