Azobisisobutyronitrile → HCID 131718421, compound

HRID 1109045Notes

Reaction equation

HRID 1109045 reaction equation
[CH2:1]([C:13](=[CH2:17])[C:14]([NH2:16])=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:18]=[CH:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1.N(C(C)(C)C#N)=NC(C)(C)C#N>C(OCC)(=O)C>[CH2:1]([C:13](=[CH2:17])[C:14]([NH2:16])=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:18]=[CH:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1

Participants

5

Reactant 3

HCID 6547AzobisisobutyronitrileHCID 7501StyreneHCID 21275882HCID 21275882, compound

Product 1

HCID 131718421HCID 131718421, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Conditions

Temperature
77 °C

Procedure

Into a reactor provided with a central stirrer and nitrogen bubbler 293.3 g of dodecylacrylamide, 6.7 g of styrene, 150 g of ethyl acetate and 0.75 g of azobisisobutyronitrile initiator are introduced. The mixture is dissolved with stirring and nitrogen bubbling, and it is then heated to 77° C. The polymerization is carried out at this temperature, with stirring and nitrogen bubbling, for 20 hours.

Workup

  1. customInto a reactor provided with a central stirrer
  2. dissolutionThe mixture is dissolved
  3. stirringwith stirring

Sources & evidence

ORD record
ord-ea5137e9beac47c0886bc8bac964aeef
Source dataset
uspto-grants-1994_06
Patent number
US05318995

Reaction notes

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