反应详情

A mixture of 153 g (1.43 mol) freshly distilled N-methylaniline, 200 g (1.46) 6-chlorohexanol, 200 g (1.45 mol) potassium carbonate, 6 g potassium iodide, and 750 mL n-butanol was heated at reflux under nitrogen with vigorous mechanical stirring for 4 days. The solution was cooled, filtered, and the solvent was removed at reduced pressure. The residue was distilled in vacuo to produce a colorless oil.

1. temperaturewas heated
2. temperatureat reflux under nitrogen with vigorous
3. temperatureThe solution was cooled
4. filtrationfiltered
5. customthe solvent was removed at reduced pressure
6. distillationThe residue was distilled in vacuo
7. customto produce a colorless oil