Hydrochloric Acid → HCID 4737568, compound
Reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:8]1(=[O:15])[CH2:13][CH2:12][C:11](=O)[CH2:10][CH2:9]1.Cl>>[OH:7][C:1]1[CH:6]=[CH:5][C:4]([C:1]2([C:11]3[CH:10]=[CH:9][C:8]([OH:15])=[CH:13][CH:12]=3)[CH2:6][CH2:5][C:4]([C:11]3[CH:12]=[CH:13][C:8]([OH:15])=[CH:9][CH:10]=3)([C:4]3[CH:5]=[CH:6][C:1]([OH:7])=[CH:2][CH:3]=3)[CH2:3][CH2:2]2)=[CH:3][CH:2]=1Participants
4
Procedure
Into a molten mixture of 300 g (3.2 mole) of phenol and 22.4 g (0.2 mole) of 1,4-cyclohexanedione (m.p. 78° C.) was introduced hydrochloric acid gas at a temperature of 50° C. to saturation.
Sources & evidence
- ORD record
- ord-d34aad80683d4124b1d8cf6637cead72
- Source dataset
- uspto-grants-1994_06
- Patent number
- US05324618
Reaction notes
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