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HRID1111089

反应详情

EQUATION

反应方程式

HRID 1111089 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

结构：BrCc1ccc(-c2nc3ccccc3o2)cc1
HCID11033515

4-(benzoxazol-2-yl)benzyl bromide

C14H10BrNO

PRODUCTS

生成物

1
结构：Cc1ccc(-c2nc3ccccc3o2)cc1[P+](c1ccccc1)(c1ccccc1)c1ccccc1.[Br-]
HCID86744426

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

A stirred solution of 172.7 g (0.6 mole) of 2-(4-bromomethylphenyl)benzoxazole and 157.4 g (0.6 mole) of triphenylphosphine in xylene is heated at reflux for 19 hours. The product is then isolated by filtration, washed with additional portions of xylene, and dried.

WORKUP

后处理

  1. temperatureat reflux for 19 hours
  2. customThe product is then isolated by filtration
  3. washwashed with additional portions of xylene
  4. customdried