Methane → HCID 22152212, compound

HRID 1111348Notes

Reaction equation

HRID 1111348 reaction equation
[Cl:1][C:2]1[CH:17]=[CH:16][C:15]([N+:18]([O-])=O)=[CH:14][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][C:9]([Cl:12])=[CH:8][C:7]=1[Cl:13])=[O:5].C>C(OCC)(=O)C>[NH2:18][C:15]1[CH:16]=[CH:17][C:2]([Cl:1])=[C:3]([CH:14]=1)[C:4]([C:6]1[CH:11]=[CH:10][C:9]([Cl:12])=[CH:8][C:7]=1[Cl:13])=[O:5]

Participants

4

Reactant 2

HCID 297MethaneHCID 15072475(2-Chloro-5-nitrophenyl)(2,4-dichlorophenyl)methanone

Product 1

HCID 22152212HCID 22152212, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

7.5 g of 2,2',4'-trichloro-5-nitrobenzophenone in 100 ml of ethyl acetate are hydrogenated at atmospheric pressure and at ambient temperature in the presence of palladinized charcoal.

Sources & evidence

ORD record
ord-7bc2e744ff4b4d7896532da3d8d888fd
Source dataset
uspto-grants-1990_12
Patent number
US04980349

Reaction notes

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