HRID1154021

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID313

Hydrochloric Acid

ClH

HCID702

Ethanol

C2H6O

HCID13365600

未命名化合物

PRODUCTS

生成物

结构：Cl.Cl.Cl.Cl.O.c1nnc2c3c(c(NCCCN4CCCC4)nn12)CCCC3.c1nnc2c3c(c(NCCCN4CCCC4)nn12)CCCC3

HCID70503725

未命名化合物

PROCEDURE

实验过程

The amine obtained above was dissolved in ethanol and treated with an excess of ethereal hydrogen chloride. The solid which formed was separated by filtration to give 6-[3-(1-pyrrolidinyl)propylamino]-7,8,9,10-tetrahydro-1,2,4-triazolo[3,4-a]phthalazine dihydrochloride hemihydrate melting at about 277°-278° C.

WORKUP

后处理

customThe solid which formed
customwas separated by filtration