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HRID1154568

反应详情

EQUATION

反应方程式

HRID 1154568 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCCO
HCID76646

1-Propanol, 3-(dimethylamino)-

C5H13NO

结构：CN(C)C(N)=S
HCID3034192

1,1-Dimethyl-2-thiourea

C3H8N2S

PRODUCTS

生成物

1
结构：CN(C)CCCSC(=N)N(C)C
HCID86120174

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Br
溶剂HCID260

Hydrogen Bromide

BrH

PROCEDURE

实验过程

A mixture of 3-dimethylaminopropanol (10.3 g), N,N1 -dimethylthiourea (10.4 g) and aqueous hydrobromic acid (48%, 60 ml) was boiled under reflux for 18 hours and evaporated to dryness. The residue was recrystallised from ethanol to give the dihydrobromide of the title compound m.p. 173°-174°.

WORKUP

后处理

  1. temperatureunder reflux for 18 hours
  2. customevaporated to dryness
  3. customThe residue was recrystallised from ethanol