反应详情

To a solution of 30 g (86.5 mmoles) of 2-chloro-1-(p-chlorophenylsulfonyl)ethyl phenyl sulfide in 100 ml of tetrahydrofuran was added 12.2 ml (8.88 g, 87.8 mmoles) of triethylamine. After two hours the reaction mixture was filtered to remove triethylamine hydrochloride. The filtrate was evaporated down under reduced pressure, first at 15 mm and finally at 0.01 mm (25° C.), to give a light yellow oil.

1. filtrationAfter two hours the reaction mixture was filtered
2. customto remove triethylamine hydrochloride
3. customThe filtrate was evaporated down under reduced pressure, first at 15 mm and finally at 0.01 mm (25° C.)
4. customto give a light yellow oil