4-Bromoaniline → HCID 28456838, compound

HRID 1158212Notes

Reaction equation

HRID 1158212 reaction equation
Br[C:2]1[CH:8]=[CH:7]C(N)=[CH:4][CH:3]=1.[Br:9][C:10]1[CH:16]=[CH:15][CH:14]=[CH:13][C:11]=1[NH2:12].C1(=O)CCCCC1>CCC(=O)CC>[Br:9][C:10]1[CH:16]=[CH:15][CH:14]=[CH:13][C:11]=1[NH:12][CH:2]([CH2:8][CH3:7])[CH2:3][CH3:4]

Participants

5

Reactant 3

HCID 78074-BromoanilineHCID 7967CyclohexanoneHCID 119922-Bromoaniline

Product 1

HCID 28456838HCID 28456838, compoundYield 61%

Reagents, catalysts & solvents 1

HCID 7288Ethyl ketoneSolvent

Procedure

The same procedure was carried out as in Example 2 except that 4-bromoaniline and 3-pentanone were used instead of 2-bromoaniline and cyclohexanone to obtain a colorless oil compound (61%).

Sources & evidence

ORD record
ord-11e802cb91ab4369be722536d48bf718
Source dataset
uspto-grants-2010_10
Patent number
US07807762B2

Reaction notes

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