Hydrochloric Acid → HCID 20512452, compound

HRID 1164460Notes

Reaction equation

HRID 1164460 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][CH2:9][CH:10]([NH:12][C:13]2[C:18]([CH3:19])=[CH:17][CH:16]=[CH:15][C:14]=2[CH3:20])[CH3:11])=[CH:4][CH:3]=1.CC1C=CC=C(C)[C:23]=1[NH2:24].Cl>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:9][CH:10]([CH3:11])[N:12]([C:13]3[C:18]([CH3:19])=[CH:17][CH:16]=[CH:15][C:14]=3[CH3:20])[C:23]2=[NH:24])=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 68962,6-DimethylanilineHCID 20512458HCID 20512458, compound

Product 1

HCID 20512452HCID 20512452, compound

Procedure

1-(4'-Chlorophenyl-amino)-2-(2',6'-dimethylphenylamino)-propane, applied as starting substance, is obtained with a yield of 50.9% by reacting N-(β-chlorophenyl)-4-chloro-aniline, a compound prepared as described in Example 27, point (b), with 2,6-dimethylaniline according to the method given in Example 25, point (a). The hydrochloride of the product melts at 170°-178° C.

Workup

  1. customis obtained with a yield of 50.9%
  2. customa compound prepared

Sources & evidence

ORD record
ord-a0917c9959af4200b4fef77f5ba49802
Source dataset
uspto-grants-1983_01
Patent number
US04369325

Reaction notes

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