HRID1166736

反应详情

EQUATION

反应方程式

HRID 1166736 的结构方程式

PROCEDURE

实验过程

4-Bromomethylnaphthoic acid (16 g, 160 mmol) in an aqueous solution of K2CO3 (10%, 100 mL) was stirred at 70° C. for 30 minutes. The reaction mixture was cooled and made acidic with conc. HCl. The resulting precipitate was filtered and dried to give the desired product as a yellow solid in quantitative yield.

WORKUP

后处理

  1. temperatureThe reaction mixture was cooled
  2. filtrationThe resulting precipitate was filtered
  3. customdried