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HRID1170011

反应详情

EQUATION

反应方程式

HRID 1170011 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(N)c(N)c1
HCID10332

3,4-Diaminotoluene

C7H10N2

结构：COC(=O)CC(=O)Nc1cnccc1C(=O)O
HCID12988781

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc2nc(-c3c(O)c4ccncc4[nH]c3=O)[nH]c2c1
HCID135518153

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized as described in Example 50 using 3-[2-(methoxycarbonyl)acetylamino]-pyridine-4-carboxylic acid and 4-methyl-1,2-phenylenediamine. The crude product was purified by reversed-phase HPLC (DMSO/5% TFA). LC/MS m/z 293.3 (MH+), Rt 1.99 minutes.

WORKUP

后处理

  1. customThe crude product was purified by reversed-phase HPLC (DMSO/5% TFA)