Lithium hydroxide, monohydrate → HCID 18409065, compound

HRID 1174214Notes

Reaction equation

HRID 1174214 reaction equation
[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][CH2:9][C:10]([O:12]CC)=[O:11])=[CH:4][CH:3]=1.O.[OH-].[Li+]>C1COCC1.O>[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][CH2:9][C:10]([OH:12])=[O:11])=[CH:4][CH:3]=1

Participants

5

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 461466324015-97-2

Product 1

HCID 18409065HCID 18409065, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
25 °C

Procedure

A solution containing ethyl 6-methyl-3-pyridyloxyacetate (0.026 g, 0.13 mmol) in a mixture of THF (0.5 mL) and water (0.5 mL) was treated with lithium hydroxide monohydrate (0.008 g, 0.19 mmol), stirred at 25° C. for 18 hours, aid concentrated to give the crude product, which was used without purification.

Workup

  1. concentrationaid concentrated

Sources & evidence

ORD record
ord-edaf472e97534fa7ac18fb1122352eec
Source dataset
uspto-grants-2010_11
Patent number
US07834043B2

Reaction notes

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