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HRID1174377

反应详情

EQUATION

反应方程式

HRID 1174377 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)[C@@H](NS(C)(=O)=O)C(C)(C)C
HCID86599586

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)[C@H](NS(C)(=O)=O)C(=O)O
HCID61142133

未命名化合物

收率 106.4%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

A solution of Example 152A (59 mg, 0.22 mmol) in 4N HCl in dioxane (1 mL) at 25° C. for 4 h, and the solvents were evaporated to give the crude title compound (49 mg, 100%).

WORKUP

后处理

  1. customthe solvents were evaporated