反应详情

Indole-3-acetic acid (3.5 g, 20 mmol) was dissolved in ethanol (70 Cm3) and a solution of hydrogen chloride in diethyl ether (12 cm3, 12 mmol) was added. The reaction was heated to reflux for 5 hand upon cooling the solvent was removed under reduced pressure to provide ethyl indole-3-acetate (4 g, 19 mmol, 98%) as a yellow oil.

1. temperatureThe reaction was heated
2. temperatureto reflux for 5 hand
3. temperatureupon cooling the solvent
4. customwas removed under reduced pressure